HPR-20 OEMS

for continuous analysis of evolved gases and vapours in electrochemistry

  • Model: HPR-20 OEMS
  • Manufacturer: Hiden Analytical

The Hiden HPR-20 OEMS mass spectrometry system is configured for continuous analysis of evolved gases and vapors to measure the volume, pressure, and composition of gas evolved during electrochemical processes (especially the charging, discharging, and aging of lithium batteries) as a function of potential on the real-time scale. The ultralow flow real time sampling capillary allows for connection for headspace sampling and/or connection to electrochemical cells, El-Cell for example.

Advantages

  •  High sensitivity, wide detection limit (detectable up to ppb)
  • The Hiden QIC-ulf quartz-lined ultra low flow sampling interface provides fast response times of less than 3 seconds for most common gases and vapours, including water vapour.

Applications

  • DEMS
  • Electrocatalyst Studies
  • Fuel Cell Studies
  • Cathode Studies
  • CO2 reduction
  • Lithium Ion Battery Research
Category:

The Hiden HPR-20 OEMS mass spectrometry system is configured for continuous analysis of evolved gases and vapors to measure the volume, pressure, and composition of gas evolved during electrochemical processes (especially the charging, discharging, and aging of lithium batteries) as a function of potential on the real-time scale. The ultralow flow real time sampling capillary allows for connection for head space sampling and/or connection to electrochemical cells, El-Cell for example.

The Hiden QIC-ulf quartz-lined ultra low flow sampling interface operating at up to 200°C provides fast response times of less than < 3 seconds for most common gases and vapours, including water vapour.

The standard system with 200 amu mass range has a detection capability to less than 100 parts-per-billion. The optional 3F series 300 amu system with triple-stage mass filter offers extended detection levels to 5 parts-per-billion together with enhanced contamination resistance and is recommended for applications requiring optimum abundance sensitivity and/or analyses of corrosive or condensable species.

Feature:

  • Quantitative data output in PPM, PPB or % units.
  • < 3 seconds response time to changes in gas concentrations.
  • Fast scan speeds up to 650 measurements/s for transient analysis.
  • APSI-MS soft ionisation mode for suppression of spectral fragmentation providing simplified analysis of complex mixtures.
  • New 3D data plot for viewing mass vs. electron energy and intensity.
  • New Automated spectral analysis providing peak identification and composition analysis.
  • Low dead volume, heated inlet for fast response to vapours.
  • Windows® MASsoft Professional PC software for data acquisition, data display and control of quadrupole parameters

Application

  • Differential Electrochemical Mass Spectrometry (DEMS) Analysis: Used to study electrochemical processes and identify gaseous and vapor products in real time.
  • Electrocatalyst studies: Investigates electrocatalytic materials to improve the efficiency and selectivity of electrochemical reactions.
  • Cathode Research: Develops cathode materials for fuel cells, solar cells, and other electrochemical devices.
  • CO2 reduction: Quantitatively analyzes CO2 reduction performance using different cathodes.
  • Fuel Cell Studies: Provides solutions for monitoring gas components to rapidly analyze reaction thermodynamics as a measure of electrocatalytic performance.
  • Lithium Ion Battery Research: Analyzes electrochemical gases during the charging, discharging, and aging of lithium batteries
  • SIMSAnalyser Specification
Quadrupole Mass spectrometer  
Mass range 200 amu standard.
300 amu mass range optional
Detection limit 0.1 PPM  subject to spectral interference
Mass Filter 3 stages each of 4 poles.
Dimension (WxDxH) 495x539x393mm
Windows® MASsoft Professional PC software Trend analysis display of partial pressure of up to 100 mass channels vs. time, and including

display of external signals, temperature for example

The Hiden DEMS Cell for Differential Electrochemical Mass Spectrometry

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