AirmoMEDOR automated gas chromatography device for analyzing and monitoring odorous sulfur compounds

Quantification of trace amounts of odorous sulfur compounds at ppm, ppb, and ppt levels

airmoMEDOR® is a specialized automatic gas chromatograph (autoGC) designed for the quantification of trace levels of odorous sulfur compounds, including Methyl-Mercaptan (MM), Ethyl-Mercaptan (EM), Di-Methyl-Sulfide (DMS), Di-Methyl-Di-Sulfide (DMDS), and Di-Ethyl-Sulfide (DES). The system employs electrochemical wet cell detection (MEDOR® technology) to provide accurate and continuous measurements at ppm, ppb, or ppt levels, meeting the stringent requirements for environmental analysis and emission control.

Applications

  • Environmental Monitoring: Evaluating air quality in both urban and rural areas and controlling fugitive emissions.
  • Odor Management: Implemented for odor control and deodorization processes in industrial facilities such as wastewater treatment plants, refineries, and petrochemical plants.
  • Quality Control of Pure Gases: Analysis of impurities in gases (CO₂, CH₄, H₂) to ensure compliance with quality standards.
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Operating Principle

  • Sampling and Preconcentration: The system automatically collects air samples and utilizes an absorbent trap to preconcentrate the target sulfur compounds.
  • Desorption and Injection: The preconcentrated compounds are thermally desorbed from the trap and injected into a metallic capillary column.
  • Isothermal Gas Chromatography: The column operates under isothermal conditions, allowing separation based on the distinct chemical properties of the analytes.
  • Electrochemical Wet Cell Detection: As compounds elute from the column, they are detected by a sulfur-specific detector (SSD) based on electrochemical wet cell technology. The detector generates a signal via the reaction between the electrolyte and the sulfur compounds.

Technical Specifications and Performance

  • Automation and Calibration: The system integrates an internal permeation tube for daily automatic calibration at the ppb or ppt level, ensuring high accuracy and data consistency.
  • Continuous Monitoring: Enables uninterrupted online sampling and analysis, providing real-time data with excellent stability.
  • High Sensitivity and Linearity: Detection limits are below 150 ppt for DES and DMS, and below 50 ppt for DMDS, MM, and EM; optional measurements for H₂S and SO₂ are performed at the ppb level.
  • Long-term Stability: The system maintains robust performance over 48 hours with RSD < 3% for concentration and < 0.5% for retention time, coupled with extended data storage capabilities.
  • Communication and Intelligent Control: Supports Ethernet communication, remote control, and data export via standard protocols (MODBUS, 4-20 mA, 0-10 V).

Optional Extensions and Additional Features

  • Multi-Channel Sampling: Supports up to 48 sampling channels for simultaneous analysis of multiple air streams.
  • Integrated Modeling Software: Includes a simulation module with a weather station (XXXDISP) for real-time odor/chemical impact assessment.
  • Explosion-Proof Version: Available in an explosion-proof variant that complies with ATEX, IECEx (Zone 1 and 2), and CSA C1D2 standards.
  • Calculation Modules: Provides modules for computing average values, statistical parameters, odor index (OU e/m³), and other relevant metrics.
  • Automatic Data Transfer: Facilitates data transmission through outputs of 4-20 mA, Modbus RTU/TCP-IP, or MGS1.
  • Gas Supply Options: Offers choices for nitrogen or air generators, with a 24V DC power supply and electronically controlled valves to reduce gas consumption, as well as wall-mounted enclosure (XXX934).

Analyzed Sulfur Compounds Standard Version: Methyl-Mercaptan (MM), Ethyl-Mercaptan (EM), Di-Methyl-Sulfide (DMS), Di-Methyl-Di-Sulfide (DMDS), Di-Ethyl-Sulfide (DES)

Optional Loop: H₂S and SO₂ (measured at the ppb level); additional compounds upon request: IPM, TBM, NPM, MES, 2BM, IBM, NBM

Detection Limits – DES, DMS: < 150 ppt (0.15 ppb)

– DMDS, MM, EM: < 50 ppt (0.05 ppb)

– H₂S, SO₂ (optional): < 5 ppb

Standard Measurement Range 0 – 100 ppb (other ranges available on demand)

(Calculations include: Odor Index, Total Sulfur, Total Mercaptans)

Relative Standard Deviation (RSD) – RSD < 3% for concentration (over 48 hours)

– RSD < 0.5% for retention time (over 48 hours)

Analysis Cycle Time – MM, EM, DMS, DMDS, DES: 900 seconds

– With optional H₂S and SO₂: 2400 seconds

– With additional compounds (IPM, TBM, NPM, 2BM, IBM, NBM, MES): 1800 seconds

Embedded Computer (Supervisor) – Windows® platform with LCD display

– Storage: 128 GB SSD

Linearity > 0.995 for all analytes
Communication Ethernet; supports remote control
Gas Supply Carrier Gas: Dry air or N₂ at 3 bar, ≤ 4 mL/min

CALIB Gas: Continuous flow of approximately 50 mL/min (increased to ~250 mL/min during validation)

Pneumatic Valve: 90 mL per cycle

Power Supply – Main power: 230V 60Hz or 115V 50Hz

– Automatic restart after power failure

– Power consumption: 150 VA

Dimensions & Weight Models: airmoMEDOR ppt – available with or without an integrated computer, with Peltier cooler, dryer, and CALIB unit

– Models: M53000 Trap, M53022 Trap

– Rack: 19″ (5U); Height: 222 mm; Width: 482 mm; Depth: 660 mm

– Net Weight: 22 kg

TSP airmoMEDOR

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